Full Description

1.1This test method covers the determination of organic chloride (above 1 g/g organically-bound chlorine) in crude oils, using distillation and combustion ion chromatography.

1.2This test method involves the distillation of crude oil test specimens to obtain a naphtha fraction prior to chloride determination. The chloride content of the naphtha fraction of the whole crude oil can thereby be obtained. See Section 5 regarding potential interferences.

1.3The test procedure covers the determination of organic chloride in the washed naphtha fraction of crude oil by combustion ion chromatography. Other halides can be determined but are not included in the precision statement of the test method.

1.4The values stated in SI units are to be regarded as standard. The preferred concentration units are micrograms of chloride per gram of sample.

1.4.1Exception-The values given in parentheses are for information only.

1.5Warning-Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPAs website-http://www.epa.gov/mercury/faq.htm-for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.