M00017488
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ISO DIS 22155 2014 Edition, September 18, 2014 SOIL QUALITY - GAS CHROMATOGRAPHIC DETERMINATION OF VOLATILE AROMATIC AND HALOGENATED HYDROCARBONS AND SELECTED ETHERS - STATICHEADSPACE METHOD
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Availability date: 07/14/2021
Description / Abstract:
This International Standard specifies a static headspace method
for quantitative gas chromatographic determination of volatile
aromatic and halogenated hydrocarbons and selected aliphatic ethers
in soil.
This International Standard is applicable to all types of
soil.
The limit of determination is dependent on the detection system
used and the quality of the methanol grade used for the extraction
of the soil sample.
Under the conditions specified in this International Standard
the following limits of determinations apply (expressed on basis of
dry matter):
Typical limit of determination when using GC-FID:
— Volatile aromatic hydrocarbons: 0,2 mg/kg;
— Aliphatic ethers as methyl tert.-butyl ether(MTBE) and
tert.-amyl methyl ether (TAME): 0,5 mg/kg.
Typical limit of determination when using GC-ECD:
— Volatile halogenated hydrocarbons: 0,01 mg/kg to 0,2
mg/kg.
Lower limits of determination can be achieved for some compounds
by using mass spectrometry (MS) with selected ion detection (see
Annex D).