M00000126
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ISO DIS 20163 .2 Edition, May 16, 2017 Vulcanized rubber - Determination of free sulfur by gas chromatography (GC) and high performance liquid chromatography (HPLC)
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Availability date: 07/13/2021
Description / Abstract:
This document specifies chromatographic methods for the determination of the inorganic free sulfur (Sx) not consumed during the vulcanization of the rubber.
NOTE 1 The amount of free sulfur is generally very low in a vulcanized rubber. Its direct determination by high performance liquid chromatography (HPLC) is possible, which is not the case with gas chromatography (GC) without prior derivatization.
NOTE 2 In this document “free sulfur” is used instead of “inorganic free sulfur”.
NOTE 3 The residual curing agent containing sulfur is not concerned by this measure.